rss_2.0Advances in Materials Science FeedSciendo RSS Feed for Advances in Materials Sciencehttps://sciendo.com/journal/ADMShttps://www.sciendo.comAdvances in Materials Science 's Coverhttps://sciendo-parsed-data-feed.s3.eu-central-1.amazonaws.com/6006591de797941b18f311be/cover-image.jpg?X-Amz-Algorithm=AWS4-HMAC-SHA256&X-Amz-Date=20220627T202044Z&X-Amz-SignedHeaders=host&X-Amz-Expires=604800&X-Amz-Credential=AKIA6AP2G7AKP25APDM2%2F20220627%2Feu-central-1%2Fs3%2Faws4_request&X-Amz-Signature=80f22d357f53db228afff1c186c547a719bc32c2ff60292b3d71de445521fd02200300Mathematical Model for Friction Stir Lap Welded AA5052 and SS304 Joints and Process Parameters Optimization for High Joint Strengthhttps://sciendo.com/article/10.2478/adms-2022-0001<abstract> <title style='display:none'>Abstract</title> <p>Due to the numerous challenges faced during the dissimilar welding, choosing the right process parameters and their optimization yields better results. In this context, the current investigation is focused on the optimization of process parameters. Taguchi’s L<sub>9</sub> orthogonal array was selected to carry out the experimental investigations. The welded samples were tested for shear strength, and the results were analysed using Taguchi’s S/N ratio analysis with “larger the better” criteria. Log-linear regression analysis was applied to formulate an empirical correlation between the process parameters and shear strength. According to S/N ratio analysis, the tool rotational speed of 800 rpm, welding speed of 20 mm/min and a penetration depth of 4.1 mm are the optimized parameters that achieve high joint strength. The achieved joint strength was 3.46 kN that is 70% of the base aluminium metal. It was noticed from the Analysis of variance of the regression model that penetration depth and tool rotational speed are the significant contributors with p-values less than 0.5. Confirmation tests show that the error between the predicted and calculated shear strength is 2.06% which is considered acceptable. R<sup>2</sup> and adjusted R<sup>2</sup> values of the model with a standard error of 0.076 show that the developed model is statistically significant.</p> </abstract>ARTICLE2022-04-05T00:00:00.000+00:00NiO/CuO/TiO Ternary Composites: Development, Physicochemical Characterization and Photocatalytic Degradation Study Over Reactive Orange 30 Solutions Under Solar Light Irradiationhttps://sciendo.com/article/10.2478/adms-2022-0003<abstract> <title style='display:none'>Abstract</title> <p>The photocatalytic degradation and mineralization of Reactive Orange 30 on NiO/CuO/TiO<sub>2</sub> ternary composites have been studied using solar light irradiation. The NiO/CuO/TiO<sub>2</sub> ternary composites were prepared by producing ethanolic dispersions containing varied amounts of NiO and CuO/TiO<sub>2</sub> (3wt% to 15wt.%), followed by annealing at 300 °C. SEM, UV- Vis DRS, PL, XRD and FTIR analysis have been used to characterize the unary (parent photocatalysts), binary and ternary composites. Under solar light irradiation, NiO/CuO/TiO<sub>2</sub> ternary composites exhibited an excellent photocatalytic activity in degradation of reactive orange 30 in aqueous solution, whereas the NiO/TiO<sub>2</sub>, CuO/TiO<sub>2</sub> and bare photocatalyst such as NiO, CuO, TiO<sub>2</sub> showed lower activities. It was deduced that the remarkable visible-light absorption phenomenon and band gap reduction of the NiO/CuO/TiO<sub>2</sub> ternary composites taking place. It paves way for the photogenerated electron transfer between CB of the NiO, CuO, TiO<sub>2</sub> semiconductors and also holes shifting between VB of above mentioned materials. The NiO/CuO/TiO<sub>2</sub> ternary composite shows good photostability and the photocatalyst retains 94% of its initial activity in the seventh cycle, respectively.</p> </abstract>ARTICLE2022-04-05T00:00:00.000+00:00Rubber Influence on the Performance of Thermal Insulating Quarry Sand Mortars-A Statistical Analysishttps://sciendo.com/article/10.2478/adms-2022-0002<abstract> <title style='display:none'>Abstract</title> <p>The purpose of this paper is to develop a framework for managing wastes resulting from the tire rubber valorization waste of quarry sand mortar. A research methodology was developed to achieve the abovementioned main objective. To create a framework for use of crumb rubber in the production of quarry sand mortars, with adequate physical and mechanical properties to be used in a variety of construction applications. Testing included strength and thermal conductivity properties of the various mixture composition subjected to varying by 5%. 10%. 15% and 20% by quarry sand substitution. The internal microstructure, and phase composition of all mixture mortars, were investigated using scanning electron microscopy and energy-dispersive X-ray spectroscopy (SEM/EDS). The results show that increasing incorporation rate of additives significantly improves thermophysical properties of based materials, the hardened properties of the various mortars made are analyzed and compared, the experimental results revealed that; the addition of crumb rubber waste in the quarry sand mortar is beneficial for physical properties (Mv) mass loss, The results of mechanics strength of the rubber based quarry mortar studied are also significantly reduced.The addition of 5% to 20% rubber crumb in matrix and the replacement of sand by 20% of rubber in quarry mortar record the low thermal conductivity properties including that appropriate QS and CR levels may change the pattern of quarry sand mortar. witch explain by a Larger pore and higher porosity produce a less rigid and uniform matrix, meaning that the sonic pulses must travel through longer and more miscellaneous paths which improvement of insulation. The good performance of new materials encourages us to integrate them into the building envelope.</p> </abstract>ARTICLE2022-04-05T00:00:00.000+00:00Chemical characteristics of new nanopowder of titania doped with nitrogen atomshttps://sciendo.com/article/10.2478/v10077-009-0013-1<abstract xml:lang="en"><title style='display:none'>Chemical characteristics of new nanopowder of titania doped with nitrogen atoms</title><p>Characteristics of new nitrogen doped TiO<sub>2</sub> prepared in an one-pot synthesis where titania (IV) complexes with ligands containing nitrogen atoms were used as a precursor are presented in this paper. The pale yellow nanopowder with crystallite size of 9 - 12 nm is obtained as a product of calcination at 310°C and repeated washing procedure. Elemental analysis shows that nitrogen (1.087 at. pct.) is present in obtained material. The morphology and microstructure of samples were examined by XRD, AFM, UV-VIS and FTIR-ATR techniques. These studies confirm that obtained powder demonstrates a significant decrease in the band gap energy value (<italic>E</italic><sub>g</sub> = 2.83 eV) comparing to pure TiO<sub>2</sub> (<italic>E</italic><sub>g</sub> 3.22 eV). Presence of N-Ti-O bonds was confirmed <italic>via</italic> FTIR ATR. Products of the powder thermal decomposition were detected using TG-DSC technique coupled with mass spectrometry (MS). The report presents electrochemical studies which allow estimation of a flatband potential <italic>E</italic><sub>fb</sub> on the basis of the Mott-Schottky relation.</p></abstract>ARTICLE2010-01-13T00:00:00.000+00:00Mathematical modelling of the thermal cycle in affected zone with three dimensional heat source models and pulsed power welding: Part IIhttps://sciendo.com/article/10.2478/v10077-009-0012-2<abstract xml:lang="en"><title style='display:none'>Mathematical modelling of the thermal cycle in affected zone with three dimensional heat source models and pulsed power welding: Part II</title><p>In order to execute computer calculations with temperature dependent physical parameters: λ, c<sub>p</sub>, ρ, a and pulsed heat input q(t), the algebraic expression will be transformed. For this purpose we will use calculations in Mathcad programme [1]. This application is very useful for modelling and simulation of welding thermal process. Finally, the specifications of sub-procedures: Stab_time, last, calculation of roots r<sub>i</sub>, λ(T), a(T) and q(t) are presented.</p></abstract>ARTICLE2010-01-13T00:00:00.000+00:00Optoelectronic system for investigation of CVD diamond/DLC layers growthhttps://sciendo.com/article/10.2478/v10077-009-0015-z<abstract xml:lang="en"><title style='display:none'>Optoelectronic system for investigation of CVD diamond/DLC layers growth</title><p>Development of the optoelectronic system for non-invasive monitoring of diamond/DLC (Diamond-Like-Carbon) thin films growth during μPA ECR CVD (Microwave Plasma Assisted Electron Cyclotron Resonance Chemical Vapour Deposition) process is described. The system uses multi-point Optical Emission Spectroscopy (OES) and long-working-distance Raman spectroscopy. Dissociation of H<sub>2</sub> molecules, excitation and ionization of hydrogen atoms as well as spatial distribution of the molecules are subjects of the OES investigation. The most significant parameters of the deposited film like molecular composition of the film can be investigated by means of Raman spectroscopy. Results of optoelectronic investigation will enable improvement of CVD process parameters and synthesized DLC films quality.</p></abstract>ARTICLE2010-01-13T00:00:00.000+00:00Allergies to implant metal compoundshttps://sciendo.com/article/10.2478/v10077-009-0014-0<abstract xml:lang="en"><title style='display:none'>Allergies to implant metal compounds</title><p>The surgical implants are made of different materials, such as cobalt alloys, titanium alloys and stainless steels. These materials contain little amount of carbon and significant amount of Cr, Ni and Mo. The metallic implants introduced into the human body undergo degradation mainly as a result of corrosion after a long use, due to aggressive biological impact between the implant surface and human body. This phenomenon is accompanied by the release of metal ions from implant surface, which gather in tissues surrounding the implant as well as the soft tissues (for eg. the liver).</p></abstract>ARTICLE2010-01-13T00:00:00.000+00:00Microstructural Characterization of Borided Co-Cr-Mo Alloyhttps://sciendo.com/article/10.2478/adms-2021-0027<abstract> <title style='display:none'>Abstract</title> <p>This study involves the effect of boriding powder composition on the microstructure and hardness of a CoCrMo alloy borided in a solid medium using the powder pack method. To investigate the effect of boriding powder composition, two different commercial boriding agents, Ekabor-HM and Ekabor III, were thoroughly mixed with ferrosilicon powders to form the boriding media. The CoCrMo samples were tightly packed with the Ekabor-HM and Ekabor III boriding powders in stainless steel containers to minimize oxidation. The boriding process was carried out under atmospheric conditions for 9 h in an electrical resistance furnace preheated to 1223 K. X-ray diffraction (XRD) analyses revealed that the surfaces of the borided CoCrMo alloys consisted of a bilayer composed of CoB and Co<sub>2</sub>B phases and also contained minor amounts of CrB, Mo<sub>2</sub>B<sub>5</sub>, and Mo<sub>2</sub>B. The average thickness of the boride layer in the samples borided with Ekabor HM and Ekabor III powders was 28±4.1 μm and 21±2.3 μm, while the average hardness of the boride layer was 1752±5.3 HV<sub>0.1</sub> and 1364±3.8 HV<sub>0.1</sub>, respectively.</p> </abstract>ARTICLE2021-12-30T00:00:00.000+00:00Effect of Fe-Ni Substitution in FeNiSiB Soft Magnetic Alloys Produced by Melt Spinninghttps://sciendo.com/article/10.2478/adms-2021-0026<abstract> <title style='display:none'>Abstract</title> <p>Alloys of FeNiSiB soft magnetic materials containing variable Fe and Ni contents (wt.%) have been produced by melt spinning method, a kind of rapid solidification technique. The magnetic and structural properties of FeNiSiB alloys with soft magnetic properties were investigated by increasing the Fe ratio. X-ray diffraction analysis and SEM images shows that the produced alloy ribbons generally have an amorphous structure, together with also partially nanocrystalline regions. It was observed that the structure became much more amorphous together with increasing Fe content in the composition. Among the alloy ribbons, the highest saturation magnetization was obtained as 0.6 emu/g in the specimen with 50 wt.% Fe. In addition, the highest Curie temperature was observed in the sample containing 46 wt.% Fe.</p> </abstract>ARTICLE2021-12-30T00:00:00.000+00:00Microstructural Evaluation of the High-Frequency Induction Welded Joints of Low Carbon Steel Pipeshttps://sciendo.com/article/10.2478/adms-2021-0022<abstract> <title style='display:none'>Abstract</title> <p>The work presents the results of research on the structure of welded joints in the area of heat affected zone (HAZ). Based on precisely performed metallographic tests, the contribution of individual structural components in the area of welds of pipes welded with the induction method was assessed. The volume fraction of individual structural components in various areas of the heat affected zone, the size of the grain formed in the welding process, as well as its shape coefficients were determined. On the basis of metallographic observations, an attempt was made to describe the course of the pressure induction welding process, taking into account the structural changes, phase changes and the recovering and recrystallization processes taking place in this process.</p> </abstract>ARTICLE2021-12-30T00:00:00.000+00:00Assessment of Corrosive Behaviour and Microstructure Characterization of Hybrid Friction Stir Welded Martensitic Stainless Steelhttps://sciendo.com/article/10.2478/adms-2021-0025<abstract> <title style='display:none'>Abstract</title> <p>This study examined the effect of induction heating on the microstructure and corrosion characteristics of hybrid friction stir welded AISI 410 stainless steel. Five joints have been produced with different friction stir welding parameters like welding speed, spindle speed, plunge depth, and induction power. Their microstructures were evaluated using a scanning electron microscope, and chemical composition was examined using energy-dispersive X-ray spectroscopy (EDX). The rate of corrosion was found out via the weight loss method in a 1 M HCL solution. The hybrid friction stir welding method used for this work is induction assisted friction stir welding; the results show that this method could produce sound AISI 410 stainless steel Joints. The experiment results show that the joint made at a spindle speed of 1150 rpm, welding speed 40 mm/min, plunge depth 0.5 mm, and in-situ heat by induction 480°C show a better corrosion resistance property with a fine grain structure.</p> </abstract>ARTICLE2021-12-30T00:00:00.000+00:00Preparation and Evaluation of Conductive Polymeric Composite from Metals Alloys and Graphene to Be Future Flexible Antenna Devicehttps://sciendo.com/article/10.2478/adms-2021-0023<abstract> <title style='display:none'>Abstract</title> <p>Every year hundreds of serious accidents and catastrophic are accompanied by mining sector services as disaster, flooding, and demolition. To reduce the severity of the results such as high death numbers, lost communication inner and out mining, we have to find an easy way to improve communication means during that problems. In this paper, we reach out to fabricate durable, flexible, and wearable chaps, in addition to an easier carrier with highly efficient receiving and sending a signal at 2.4 GHz broad wide band. By doping a bunch of unique conductive metals (silver, copper, and gallium indium alloy) assembled on Graphene, its integration inside Polydimethylsiloxane to be future applicable antenna. Furthermore, we studied the physical and electric properties of a composite including Electrochemical Impedance properties (EIS), cyclic voltammetry (CV), and its thermal stability chip (DSC), as well as, using Transmission electron microscopy (TEM), and, scanning electron microscopy (SEM) techniques to clarify the surface morphology of fabricated materials. In addition to various measurements had been carried out such as Ultraviolet-visible, inductively coupled plasma (ICP) spectroscopy, and Energy-dispersive X-ray spectroscopy (EDX) to reinforce and elucidate the solid-state of ions inside fabricated Antenna. On the other hand, throughout stress-strain for the stretchability of fabricated is expanded to 30% of its original length, in addition to thermal stability reached to 485°C compared to pure PDMS substrate, with enhancing electric conductivity of composite ship.</p> </abstract>ARTICLE2021-12-30T00:00:00.000+00:00Microstructure and Mechanical Properties of Laser Surface-Treated Ti13Nb13Zr Alloy with MWCNTs Coatingshttps://sciendo.com/article/10.2478/adms-2021-0021<abstract> <title style='display:none'>Abstract</title> <p>Laser surface modification of titanium alloys is one of the main methods of improving the properties of titanium alloys used in implantology. This study investigates the microstructural morphology of a laser-modified surface layer on a Ti13Nb13Zr alloy with and without a carbon nanotube coating deposited by electrophoretic deposition. Laser modification was performed for samples with and without carbon nanotube coating for two different laser powers of 800 W and 900 W and for different scan rates: 3 mm/s or 6 mm/s at 25 Hz, and the pulse duration was 2.25 ms or 3.25 ms. A scanning electron microscope SEM was used to evaluate the surface structure of the modified samples. To observe the heat-affected zones of the individual samples, metallographic samples were taken and observed under an optical microscope. Surface wettability tests were performed using a goniometer. A surface roughness test using a profilograph and a nanoindentation test by NanoTest™ Vantage was also performed. Observations of the microstructure allowed to state that for higher laser powers the surfaces of the samples are more homogeneous without defects, while for lower laser powers the path of the laser beam is clearer and more regular. Examination of the microstructure of the cross-sections indicated that the samples on which the carbon nanotube coating was deposited are characterized by a wider heat affected zone, and for the samples modified at 800 W and a feed rate of 3 mm/s the widest heat affected zone is observed. The wettability tests revealed that all the samples exhibit hydrophilic surfaces and the samples with deposited carbon nanotube coating increase it further. Surface roughness testing showed a significant increase in Ra for the laser-modified samples, and the presence of carbon nanotubes further increased this value. Nanoindentation studies showed that the laser modification and the presence of carbon coating improved the mechanical properties of the samples due to their strength.</p> </abstract>ARTICLE2021-12-30T00:00:00.000+00:00The Effect of Spray Distance on Porosity, Surface Roughness and Microhardness of WC-10Co-4Cr Coatings Deposited by HVOFhttps://sciendo.com/article/10.2478/adms-2021-0028<abstract> <title style='display:none'>Abstract</title> <p>The paper presents the computational studies on the microstructure of WC-Co-Cr coatings deposited by High Velocity Oxy Fuel spraying (HVOF). The study covers the porosity assessment according to ASTM E2109-01 standard, carried out in ImageJ software, in terms of volume porosity, size and shape of the pores. The evaluation was preceded by scanning electron microscope (SEM) observations at magnifications of 2000x and 5000x. Additionally, topography analysis has been performed by confocal laser scanning microscope (CLSM), and the surface roughness R<sub>a</sub> was evaluated by the contact method with use of a stylus profilometer. Finally, the influence of porosity was observed for coatings microhardness HV0.3. According to the results, the total closed porosity was found to be in the range of 5.01 vol.% and 5.38 vol.%. The dominated pores in the coatings were of size 0.1-1.0 μm. Studies showed that HVOF process enabled deposition of dense coatings, characterized by homogenous distribution of pores and low roughness.</p> </abstract>ARTICLE2021-12-30T00:00:00.000+00:00Effect of Holes in Overlap on the Load Capacity of the Single-Lap Adhesive Joints Made of EN AW-2024-T3 Aluminium Alloyhttps://sciendo.com/article/10.2478/adms-2021-0029<abstract> <title style='display:none'>Abstract</title> <p>The paper presents the results of experimental research aimed at determining the possibilities of strengthening structural adhesive joints. Techniques to improve the strength of adhesive joints was to make holes in the front part of the adherends in order to make the joint locally more flexible in the area of stress concentration at the joint edges. The tests were carried out for the lap joints of EN AW-2024-T3 aluminum alloy sheets, which were bonded with Loctite EA3430 epoxy adhesive. Static tests were carried out on the basis of the tensile/shear test. It has been shown that the applied structural modifications allow for an increase in the strength of the joint, in the best variant, an increase in strength of 14.5% was obtained. In addition, it has been shown that making holes in the adherends allows to reduce the spread of strength results.</p> </abstract>ARTICLE2021-12-30T00:00:00.000+00:00Physico-Mechanical and Thermal Properties of Thermoplastic Poly(Vinyl Alcohol) Modified Thermosetting Urea Formaldehyde Resinhttps://sciendo.com/article/10.2478/adms-2021-0024<abstract> <title style='display:none'>Abstract</title> <p>Urea formaldehyde (UF) resins are brittle and to improve their tensile properties poly(vinyl alcohol) (PVA) has been used to modify the UF resin. An easy improved procedure was developed to make PVA modified UF resin on the basis of conventional synthesis of UF resin. Prepolymer of UF was mixed with different weight percentages of PVA (1-5%) to synthesize modified UF resin which can be used to make adhesive for forest products. Both UF and modified UF resins were characterized by FTIR, physico-mechanical and thermal properties analyses. Modified UF resin containing 2 wt. % PVA exhibited better results than the UF.</p> </abstract>ARTICLE2021-12-30T00:00:00.000+00:00Induction Assisted Hybrid Friction Stir Welding of Dissimilar Materials AA5052 Aluminium Alloy and X12Cr13 Stainless Steelhttps://sciendo.com/article/10.2478/adms-2021-0015<abstract> <title style='display:none'>Abstract</title> <p>This research aimed to study the induction <italic>in-situ</italic> heated hybrid friction stir welding (IAFSW) method to join AA5052 aluminium alloy with X12Cr13 stainless steel (SS) to enhance joint strength. The potency of this method on the mechanical properties and microstructural characterizations were also investigated. The results show that the transverse tensile strength gained was 94% of the AA5052 base metal that is 229.5 MPa. This superior strength was achieved due to the annealing that happened to the AA 5052 region and elevated plastic flow in the weld zone by the <italic>in-situ</italic> induction heating, which resulted in the elongation of the weld region. The microstructure characterization indicates that a refined grain structure was gained in the nugget zone without defects.</p> </abstract>ARTICLE2021-10-05T00:00:00.000+00:00Modelling Anisotropic Phenomena of Friction of Deep-Drawing Quality Steel Sheets Using Artificial Neural Networkshttps://sciendo.com/article/10.2478/adms-2021-0016<abstract> <title style='display:none'>Abstract</title> <p>This paper presents a method of determining the coefficient of friction in metal forming using multilayer perceptron based on experimental data obtained from the pin-on-disk tribometer. As test material, deep-drawing quality DC01, DC03 and DC05 steel sheets were used. The experimental results show that the coefficient of friction depends on the measured angle from the rolling direction and corresponds to the surface topography. The number of input variables of the artificial neural network was optimized using genetic algorithms. In this process, surface parameters of the sheet, sheet material parameters, friction conditions and pressure force were used as input parameters to train the artificial neural network. Some of the obtained results have pointed out that genetic algorithm can successfully be applied to optimize the training set. The trained multilayer perceptron predicted the value of the friction coefficient for the DC04 sheet. It was found that the tested steel sheet exhibits anisotropic tribological properties. The highest values of the coefficient of friction under dry friction conditions were registered for sheet DC05, which had the lowest value of the yield stress. Prediction results of coefficient of friction by multilayer perceptron were in qualitative and quantitative agreement with the experimental ones.</p> </abstract>ARTICLE2021-10-05T00:00:00.000+00:00A Review on Utilizing the Marine Biorefinery Waste in Construction Raw Materials to Reduce Land Pollution and Enhance Green Environmenthttps://sciendo.com/article/10.2478/adms-2021-0017<abstract> <title style='display:none'>Abstract</title> <p>This research mainly concentrates on eco-friendly construction material. Production of cement and concrete industries release huge amount of carbon dioxide (CO<sub>2</sub>) and greenhouse gases which affect the environment and also there is a demand in construction material by man-made or nature. The construction sector finds an economic and eco-friendly cement replacement material to achieve the demand for green concrete that improve the energy conservation and better energy saving material. In marine Bio-refinery waste produce huge quantity of calcium carbonate, whose disposal is cause of major concern. Pre-eminent solution for this problem is utilizing the marine shell waste in cement and concrete. It revises the manufacturing process to reduce the raw material usage in production and adoptable material for global warming. Therefore, the researchers focus on marine waste sea shells as the replacement material in construction industry to save the energy and also give sustainable green material. As per the previous studies by the researchers to determine the chemical composition, specific gravity, water absorption, particle size distribution of seashells and also compressive, flexural and tensile strength of concrete. It shows the seashell is filler material that slightly increases the strength when compared to the conventional materials and therefore the sea shells are suitable for the construction field to manufacture the cement and concrete with eco-friendly manner.</p> </abstract>ARTICLE2021-10-05T00:00:00.000+00:00Plasticizing Properties Improvement of Poly (4-Vinylpyridine)/Clay Composites: Effect of Composition and Clay Naturehttps://sciendo.com/article/10.2478/adms-2021-0014<abstract> <title style='display:none'>Abstract</title> <p>A significant number of investigations have been reported on the elaboration and characterization of Polymer/Clays composites, via different methods. In our work, new composites materials were successfully prepared by in-situ polymerization of 4-vinylpyridine (4VP), in presence of two different types of Algerian modified clays (Maghnia and Mostaganem), noted (BC) and (MC), respectively. Different percentage clays (1 wt%, 3 wt% and 5 wt%) have been used. The differential scanning calorimetry analysis reveals the variation of glass transition temperature (Tg) of the copolymer in the composite materials. We show a decrease glass transition temperature (Tg) from 147°C to 131°C for P4VP-BC and from 147°C to 124°C for P4VP-MC according to the increase percentage of clays. Thermogravimetric analysis (TGA) shows good stability of composite materials at high temperature. Fourier Transformed Infrared (FTIR), Scanning Electron Microscopy coupled with Energy dispersive X-Ray Spectroscopy (SEM-EDX) and <sup>1</sup>H NMR spectroscopy are used to show the presence of the clays in the materials.</p> </abstract>ARTICLE2021-10-05T00:00:00.000+00:00en-us-1